PIHKALAnthologyShulgin_page_772

PIHKALAnthologyShulgin | page 772 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

129 METHYL-K; 2-METHYLAMINO-1-(3,4- METHYLENEDIOXY PHENYL)PENTANE; N- METHYL-1-(1,3-BENZODIOXOL-S-YL)-2- PENTYLAMINE SYNTHESIS: The Grignard reagent of butyl bromide was prepared in anhydrous Et2O by the dropwise addition of 68 g n-butyl bromide to a well-stirred suspension of 14 g magnesium…