PIHKALAnthologyShulgin_page_767

PIHKALAnthologyShulgin | page 767 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

127 METHYL-DOB; 4-BROMO-2,5- DIMETHOXY-N-METHYLAMPHETAMINE SYNTHESIS: To a solution of 6.0 g of the free base of 2,5-dimethoxy-N-methyl-amphetamine (see recipe under METHYL-DMA) in 30 mL glacial acetic acid there was added, dropwise and with good stirring, a solution of 5.5 g bromine in 15 mL…