PIHKALAnthologyShulgin_page_763

PIHKALAnthologyShulgin | page 763 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

The other melted at 124.5-125.5 !C and had major fingerprint peaks at 694, 731, 839 and 897 cm-1. Anal. (C10H1203S) C,H. A solution of 8.2 g 2,4-dimethoxy-5-(methylthio)benzaldehyde in 30 mL nitroethane was treated with 1.8 g anhydrous ammonium acetate and heated on the steam bath for 4 h. Removal…