PIHKALAnthologyShulgin_page_762

PIHKALAnthologyShulgin | page 762 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

125 META-DOT; 2,4-DIMETHOXY-S- METHYLTHIOAMPHETAMINE SYNTHESIS: To 27 g 1,3-dimethoxybenzene that was being well stirred, there was added, dropwise, 29 g concentrated H2SO4 over a period of 15 min. Stirring was continued for | hour, and then the mixture was poured slowly into 250 mL of saturated…