PIHKALAnthologyShulgin_page_758

PIHKALAnthologyShulgin | page 758 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

123 MEPEA; 3-METHOXY-4- ETHOXY PHENETHYLAMINE SYNTHESIS: A solution of 10.0 g 3-methoxy-4-ethoxybenzaldehyde in 150 mL nitromethane was treated with 1.7 g anhydrous ammonium acetate, and heated on the steam bath for | h. The excess nitromethane was removed under vacuum, yielding a loose, yellow…