PIHKALAnthologyShulgin_page_755

PIHKALAnthologyShulgin | page 755 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

with an external ice bath. The excess hydride was destroyed by the cautious addition of 300 mL of 1.5 N H2S04. When the aqueous and Et2O layers were finally clear, they were separated, and 100 g of potassium sodium tartrate was dissolved in the aqueous fraction. Aqueous NaOH was then added until…