PIHKALAnthologyShulgin_page_754

PIHKALAnthologyShulgin | page 754 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

distilled as a clear oil at 180-190 !C at 0.8 mn/Hg. This product, 45.1 g, gave a fine NMR spectrum, and in dilute CCl4 showed a single OH band at 3620 cm-1, supporting the freedom of the OH group on the aromatic ring from adjacent oxygen. Efforts to obtain an NMR spectrum in D2O immediately formed…