PIHKALAnthologyShulgin_page_753

PIHKALAnthologyShulgin | page 753 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

122 MEM; 2,5-DIMETHOXY-4- ETHOXYAMPHETAMINE SYNTHESIS: A solution of 83 g bourbonal (also called ethyl vanillin, or vanillal, or simply 3-ethoxy-4- hydroxybenzaldehyde) in 500 mL MeOH was treated with a solution of 31.5 g KOH pellets (85% material) dissolved in 250 mL H20. There was then added 71 g…