PIHKALAnthologyShulgin_page_750

PIHKALAnthologyShulgin | page 750 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

121 MEE; 4,5-DIETHOXY-2- METHOXYAMPHETAMINE SYNTHESIS: To a solution of 166 g bourbonal in 1 L MeOH there was added a solution of 66 g KOH pellets in 300 mL H20. There was then added 120 g ethyl bromide, and the mixture was held at reflux on the steam bath for 3 h. The reaction was quenched with…