PIHKALAnthologyShulgin_page_745

PIHKALAnthologyShulgin | page 745 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

added slowly with continuous stirring. The white crystalline 3,4-dimethoxy-5-ethoxyphenethylamine hydrochloride (ME) was isolated by filtration, washed with Et2O, and air dried, and weighed 2.4 g. It had a mp of 202-203 !C which increased by one degree upon recrystallization from boiling IPA. Anal.…