PIHKALAnthologyShulgin_page_735

PIHKALAnthologyShulgin | page 735 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

116 MDPH; a,a-DIMETHYL-3,4- METHYLENEDIOXY- PHENETHYLAMINE; 3,4-METHYLENEDIOXYPHENTERMINE SYNTHESIS: To 150 mL of THF, under an atmosphere of nitrogen, there was added 11.2 g diisopropylamine, and the solution was cooled with external dry ice/IPA. There was then added 48 mL of a 2.3 M solution of…