PIHKALAnthologyShulgin_page_733

PIHKALAnthologyShulgin | page 733 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

115 MDPEA; 3,4- METHYLENEDIOXYPHENETHYLAMINE; HOMOPIPERONYLAMINE SYNTHESIS: A suspension of 4.0 g LAH in 300 mL anhydrous Et2O was stirred and heated to a gentle reflux in an inert atmosphere. There was added 3.9 g 3,4-methylenedioxy-'-nitrostyrene (see under BOH for its preparation) by allowing…