PIHKALAnthologyShulgin_page_731

PIHKALAnthologyShulgin | page 731 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

114 MDOH; N-HYDROXY-MDA; 3,4- METHYLENEDIOXY-N- HYDROXYAMPHETAMINE SYNTHESIS: To a well stirred solution of 14.8 g hydroxylamine hydrochloride in 120 mL MeOH there was added 3.6 g of 3,4-methylenedioxyphenylacetone (see under MDMA for its preparation) followed by 1.0 g sodium cyanoborohydride. The…