PIHKALAnthologyShulgin_page_724

PIHKALAnthologyShulgin | page 724 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

110 MDMC; EDMA; 3,4-ETHYLENEDIOXY- N-METHYLAMPHETAMINE SYNTHESIS: To a solution of 27.6 g protocatechualdehyde (3,4-dihydroxybenzaldehyde) in 250 mL acetone there was added 57 g finely powdered anhydrous K2CO3 and 43 g 1,2-dibromoethane. The mixture was held at reflux for 16 h, and then the acetone…