PIHKALAnthologyShulgin_page_720

PIHKALAnthologyShulgin | page 720 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

sufficient HCl added to make the phase distinctly acidic. This was then washed with 3x75 mL CH2C12, made basic with 25% NaOH, and extracted with 3x100 mL of CH2C12. After removal of the solvent from the combined extracts, there remained 55 g of an amber oil which was distilled at 100-110 !C at 0.4…