PIHKALAnthologyShulgin_page_712

PIHKALAnthologyShulgin | page 712 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

!C at 0.5 mm/Hg, producing 40.3 g of an off-white oil. This was dissolved in 600 mL IPA, neutralized with about 20 mL of concentrated HCI and then treated with 300 mL anhydrous Et2O. After filtering off the white crystals, washing with a IPA/Et2O (2:1) mixture, with Et2O and air drying, the final…