PIHKALAnthologyShulgin_page_697

PIHKALAnthologyShulgin | page 697 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

100 MDA; 3,4- METHYLENEDIOXYAMPHETAMINE SYNTHESIS: (from piperonal) To a solution of 15.0 g piperonal in 80 mL glacial acetic acid there was added 15 mL nitroethane followed by 10 g cyclohexylamine. The mixture was held at steam-bath temperature for 6 h, diluted with 10 mL H20, seeded with a…