PIHKALAnthologyShulgin_page_694

PIHKALAnthologyShulgin | page 694 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

99 MAL; METHALLYLESCALINE; 3,5-DIMETHOXY-4-METHALLYLOXYPHENETHYLAMINE) SYNTHESIS: To a solution of 5.8 g of homosyringonitrile (see under ESCALINE for its preparation) in 50 mL of acetone containing 100 mg of decyltriethylammonium iodide there was added 7.8 mL methallyl chloride followed by 6.9 g…