PIHKALAnthologyShulgin_page_692

PIHKALAnthologyShulgin | page 692 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

poured into 2 L dilute H2S04 (caution, HCN evolved). This was washed with 3x75 mL CH2C12, made basic with 25% NaOH, and the resulting mixture extracted with 3x100 CH2C12. The pooled extracts were stripped of solvent under vacuum and the residue, 15 g ofa pale amber oil, was distilled at 95-110 !C…