PIHKALAnthologyShulgin_page_691

PIHKALAnthologyShulgin | page 691 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

98 MADAM-6; 2,N-DIMETHYL-4,5- METHYLENEDIOXYAMPHETAMINE SYNTHESIS: A mixture of 102 g POCI3 and 115 g N-methylformanilide was allowed to stand for 0.5 h at room temperature during which time it turned a deep claret color. To this there was added 45 g 3,4- methylenedioxytoluene and the mixture was…