PIHKALAnthologyShulgin_page_682

PIHKALAnthologyShulgin | page 682 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

95 LOPHOPHINE; 3-METHOXY-4,5- METHYLENEDIOXYPHENETHYLAMINE SYNTHESIS: A solution of 50 g myristicinaldehyde (3-methoxy-4,5-methylenedioxybenzaldehyde, see under MMDA for its preparation) in 200 mL acetic acid was treated with 33 mL nitromethane and 17.4 g anhydrous ammonium acetate and held on the…