PIHKALAnthologyShulgin_page_679

PIHKALAnthologyShulgin | page 679 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

94 J; BDB; 2-AMINO-1-(3,4- METHYLENEDIOXYPHENYL)BUTANE; 1- (1,3-BENZODIOXOL-5-YL)-2-BUTANAMINE SYNTHESIS: The Grignard reagent of propyl bromide was made by the dropwise addition of 52 g 1- bromopropane to a stirred suspension of 14 g magnesium turnings in 50 mL anhydrous Et2O. After the addition,…