PIHKALAnthologyShulgin_page_675

PIHKALAnthologyShulgin | page 675 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

93 IRIS; 5-ETHOXY-2-METHOXY-4- METHYLAMPHETAMINE SYNTHESIS: To a solution of 9.5 g flaked KOH (10% excess) in 500 mL 95% EtOH there was added 20.4 g 4-methoxy-2-methylphenol (see under 2C-D for its preparation). This was followed with 23.5 g ethyl iodide, and the mixture was held at reflux…