PIHKALAnthologyShulgin_page_670

PIHKALAnthologyShulgin | page 670 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

91 IM; ISOMESCALINE; 2,3,4- TRIMETHOXYPHENETHYLAMINE SYNTHESIS: A solution of 8.0 g 2,3,4-trimethoxybenzaldehyde in 125 mL nitromethane containing 1.4 g anhydrous ammonium acetate was held at reflux for 1.5 h. The conversion of the aldehyde to the nitrostyrene was optimum at this time, with a…