PIHKALAnthologyShulgin_page_667

PIHKALAnthologyShulgin | page 667 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

90 IDNNA; 2,5-DIMETHOXY-N,N- DIMETHYL-4-IODOAMPHETAMINE SYNTHESIS: To a stirred solution of 0.4 g 2,5-dimethoxy-4-iodoamphetamine hydrochloride (DOI) in 12 mL MeOH containing 4 mL of a 40% formaldehyde solution there was added 1 g sodium cyanoborohydride. The pH was kept at about 6 by the…