PIHKALAnthologyShulgin_page_664

PIHKALAnthologyShulgin | page 664 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

89 HOT-17; 2,5-DIMETHOXY-4-(s)- BUTYLTHIO-N- HYDROXYPHENETHYLAMINE SYNTHESIS: To a well-stirred solution of 6.08 g 2,5-dimethoxy-4-(s)-butylthio-'-nitrostyrene (see under 2C-T-17 for its preparation) in 80 mL anhydrous THF under a He atmosphere, there was added 3.5 mL 10 M borane dimethylsulfide…