PIHKALAnthologyShulgin_page_662

PIHKALAnthologyShulgin | page 662 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

88 HOT-7; 2,5-DIMETHOXY-N-HYDROXY-4- (n)-PROPYLTHIOPHENETHYLAMINE SYNTHESIS: A well-stirred solution of 1.77 g 2,5-dimethoxy-'-nitro-4-(n-propylthio)styrene (see under 2C-T-7 for its preparation) in 20 mL anhydrous THF was placed in an He atmosphere and treated with 1.5 mL of 10 M borane-dimethyl…