PIHKALAnthologyShulgin_page_660

PIHKALAnthologyShulgin | page 660 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

87 HOT-2; 2,5-DIMETHOXY-4-ETHYLTHIO- N-HYDROXYPHENETHYLAMINE SYNTHESIS: A solution of 5.50 g 2,5-dimethoxy-4-ethylthio-'-nitrostyrene (see under 2C-T-2 for its preparation) was made in 80 mL boiling anhydrous THF. On cooling, there was some separation of a fine crystalline phase, which was kept…