PIHKALAnthologyShulgin_page_653

PIHKALAnthologyShulgin | page 653 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

84 G-5; 3,6-DIMETHOXY-4-(2- AMINOPROPYL)BENZONORBORNANE SYNTHESIS: A solution of 3.70 g 3,6-dimethoxy-4-formylbenzonorbornane (see under 2C-G-S for its preparation) in 20 g nitroethane was treated with 0.88 g anhydrous ammonium acetate and held at steam bath temperature overnight. The excess…