PIHKALAnthologyShulgin_page_645

PIHKALAnthologyShulgin | page 645 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

days. From the first there was obtained 1.4 g of product with a mp of 153-154 !C; from the second, 0.2 g with a mp of 153-154 !C; and from the third, 1.2 g with a mp of 155-156 !C. These crops were combined, and recrystallized from 10 mL of boiling CH3CN to give 1.7 g…