PIHKALAnthologyShulgin_page_634

PIHKALAnthologyShulgin | page 634 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

EtOH was treated with 20 g flaked KOH, and heated on the steam bath. The progress of the isomerization was followed by the assay of isolates by GC. After 5 h, the reaction mixture was poured into 250 mL H20 which immediately generated a pasty solid. This was sucked free of solvent and other liquids…