PIHKALAnthologyShulgin_page_630

PIHKALAnthologyShulgin | page 630 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

course of | h. Refluxing was maintained for 5 h and the reaction mixture was cooled with an external ice bath with the stirring continued. The excess hydride was destroyed by the cautious addition of 400 mL of 1.5 N H2S04. When the aqueous and Et2O layers were finally clear, they were separated,…