PIHKALAnthologyShulgin_page_629

PIHKALAnthologyShulgin | page 629 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

74 EEM; 2,4-DIETHOXY-5- METHOXYAMPHETAMINE SYNTHESIS: To a solution of 12.3 g 3-ethoxy-4-methoxyphenol (see recipe for MEM for the preparation of this phenol) in 20 mL MeOH, there was added a warm solution of 4.8 g KOH in 100 mL MeOH. There was then added 8.2 g ethyl bromide, and the mixture held…