PIHKALAnthologyShulgin_page_627

PIHKALAnthologyShulgin | page 627 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

73 EEE; 2,4,5-TRIETHOXYAMPHETAMINE SYNTHESIS: A solution of 13.3 g 3,4-diethoxyphenol (see the recipe for MEE for its preparation) in 20 mL MeOH, and a solution of 4.8 g KOH in 100 mL hot MeOH were combined. There was added 8.2 g ethyl bromide and the mixture was held at reflux on the steam bath…