PIHKALAnthologyShulgin_page_624

PIHKALAnthologyShulgin | page 624 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

heated to reflux in a heating mantle. There was then added a solution of 15 g NaOH in 60 mL H20. The heating and stirring was continued until the generated solids redissolved. Over a period of 10 min, there was added 23 g diethyl sulfate, then refluxing was continued for | h. Four additional…