PIHKALAnthologyShulgin_page_623

PIHKALAnthologyShulgin | page 623 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

72 E; ESCALINE; 3,5-DIMETHOXY-4- ETHOXY PHENETHYLAMINE SYNTHESIS: To a solution of 72.3 g 2,6-dimethoxyphenol in 400 mL MeOH, there was added 53.3 g of a 40% solution of aqueous dimethylamine folowed by 40 g of a 40% aqueous solution of formaldehyde. The dark solution was heated under reflux for…