PIHKALAnthologyShulgin_page_615

PIHKALAnthologyShulgin | page 615 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

69 Y-DOM; Z-7; 2,6-DIMETHOXY-4- METHYLAMPHETAMINE SYNTHESIS: To a solution of 2,6-dimethoxy-4-methylbenzaldehyde (mp 92-93 !C from the lithiation of 3,5-dimethoxytoluene followed by reaction with N-methylformanilide) in 10 mL nitroethane, there was added 0.1 g anhydrous am-monium acetate and the…