PIHKALAnthologyShulgin_page_599

PIHKALAnthologyShulgin | page 599 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

65 DOEF; 2,5-DIMETHOXY-4-(2- FLUOROETHYL)- AMPHETAMINE SYNTHESIS: A well-stirred solution of 0.45 g free base DOB in 2 mL CH2C1l2 was treated with 0.37 g triethylamine, cooled to 0 !C, and there was then added a solution of 0.39 g 1,1,4,4-tetramethyl-1,4-dichlorodisilylethylene in 2 mL CH2C12. The…