PIHKALAnthologyShulgin_page_597

PIHKALAnthologyShulgin | page 597 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

64 DOC; 2,5-DIMETHOXY-4- CHLOROAMPHETAMINE SYNTHESIS: A solution of 6.96 g 2,5-dimethoxyamphetamine hydrochloride (2,5-DMA) in 250 mL H20 was made basic with aqueous NaOH and extracted with 3x75 mL CH2C12. After removal of the solvent from the pooled extracts under vacuum, the residual free base…