PIHKALAnthologyShulgin_page_593

PIHKALAnthologyShulgin | page 593 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

63 DOBU; 2,5-DIMETHOXY-4-(n)- BUTYLAMPHETAMINE SYNTHESIS: A well stirred suspension of 140 g anhydrous AICI3 in 400 mL CH2Cl2 was treated with 102 g butyryl chloride. This mixture was added in small portions, over the course of 20 min, to a well-stirred solution of 110.4 g p-dimethoxybenzene in 300…