PIHKALAnthologyShulgin_page_588

PIHKALAnthologyShulgin | page 588 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

90% pure 2,5-dimethoxy-(n)-amylbenzene. A mixture of 36.3 g POCI3 and 40.9 g N-methylformanilide was allowed to incubate for 0.5 h. To this there was then added 18.5 g of 2,5-dimethoxy-(n)-amylbenzene and the mixture heated on the steam bath for 2 h. This mixture was poured into a large quantity of…