PIHKALAnthologyShulgin_page_581

PIHKALAnthologyShulgin | page 581 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

DMMDA homologues started with the reduction of the nitrosyrene to the ketone (see under METHYL- MMDA-2 for this preparation), followed by methylation with fresh sodium isopropoxide and methyl iodide, to give the beta-methyl product. This formed the two possible oximes, one with a mp of 120 !C, and…