
PIHKALAnthologyShulgin | page 577 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf
37 DME; 3,4-DIMETHOXY-'- HYDROXY PHENETHYLAMINE SYNTHESIS: To a solution of 10.2 g 3,4-dimethoxybenzaldehyde in 10 mL EtOH, cooled to 0 !C, there was added a solution of 4.2 g KCN in 40 mL H20. With good stirring, there was slowly added 10 mL concentrated HCl (caution: HCN is evolved) and the…