PIHKALAnthologyShulgin_page_574

PIHKALAnthologyShulgin | page 574 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

56 DMCPA; 2-(2,5-DIMETHOXY-4- METHYLPHENYL)CYCLOPROPYLAMINE SYNTHESIS: To a solution of 25 g 2,5-dimethoxy-4-methylbenzaldehyde (see the recipe for 2C-D for the preparation) and 29.2 g malonic acid in 50 mL anhydrous pyridine, there was added 2 mL piperidine and this was heated on the steam bath…