PIHKALAnthologyShulgin_page_568

PIHKALAnthologyShulgin | page 568 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

54 2,5-DMA; DMA; 2,5- DIMETHOXYAMPHETAMINE SYNTHESIS: A solution of 10.0 g 2,5-dimethoxybenzaldehyde in 50 mL glacial acetic acid was treated with 6.8 g of nitroethane and 4.0 g of anhydrous ammonium acetate. This mixture was heated on the steam bath for 3 h and then the reagent/solvent was removed…