PIHKALAnthologyShulgin_page_565

PIHKALAnthologyShulgin | page 565 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

53 2,4-DMA: 2,4- DIMETHOXYAMPHETAMINE SYNTHESIS: To a solution of 10 g 2,4-dimethoxybenzaldehyde in 50 mL nitroethane there was added 0.5 g anhydrous ammonium acetate, and the mixture was heated on the steam bath for 2 h. The excess solvent/reagent was removed under vacuum, and the residue oil…