PIHKALAnthologyShulgin_page_562

PIHKALAnthologyShulgin | page 562 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

52 DESOXY; 3,5-DIMETHOXY-4- METHYLPHENETHYLAMINE SYNTHESIS: To a well-stirred solution of 31 g 2,6-dimethoxytoluene in 200 mL CH2C12 there was added 11 mL elemental bromine, a portion at a time. There was a copious evolution of HBr and the color gradually faded from deep red to straw. The reaction…