PIHKALAnthologyShulgin_page_555

PIHKALAnthologyShulgin | page 555 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

50 4-D; 3,5-DIMETHOXY-4- TRIDEUTEROMETHOXY- PHENETHYLAMINE SYNTHESIS: To a solution of 34.0 g homosyringonitrile (3,5-dimethoxy-4-hydroxyphenylacetonitrile, see under ESCALINE for its preparation) in 350 mL acetone containing 0.5 g decyltriethylammonium iodide, there was added 25 g trideuteromethyl…