PIHKALAnthologyShulgin_page_552

PIHKALAnthologyShulgin | page 552 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

amber oil. This was dissolved in 600 mL dilute H2SO4, and washed with 3x50 mL CH2C12 (which removed the light yellow color). The aqueous phase was made strongly basic with 25% NaOH, extracted with 3x75 mL CH2C12 and, after pooling, the solvent was removed under vacuum leaving 4.91 g of product as…