PIHKALAnthologyShulgin_page_551

PIHKALAnthologyShulgin | page 551 | https://thedailydialectics.com/pdfs/education/chemistry/phenylethylenes/PIHKALAnthologyShulgin/PIHKALAnthologyShulgin.pdf

49 2C-T-21; 2,5-DIMETHOXY-4-(2- FLUOROETHYLTHIO)PHENETHYLAMINE SYNTHESIS: To a solution of 6.9 g of KOH pellets in 100 mL hot MeOH, there was added 13.0 g 2,5- dimethoxythiophenol (see under 2C-T-2 for its preparation) followed by 9.6 g 2-fluoroethyl bromide. The reaction was exothermic, with the…